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Chemistry: electrical and wave energy March listing by industry category 03/09Below are recently published patent applications awaiting approval from the USPTO. Recent week's RSS XML file available below.
Listing for abstract view: USPTO application #, Title, Abstract excerpt,Patent Agent. Listing format for list view: USPTO National Class full category number, title of the patent application. 03/26/2009 > patent applications in patent subcategories.
20090078559 - Method and apparatus for multiple resonant structure process and reaction chamber: A method and apparatus is described comprising of a plurality of electromagnetic resonant structures coupled to a common process or reaction volume, such that resonance of each structure is maintained while the process or reaction volume is a part of each resonant structure. At the same time, each resonant structure... Agent: Hayes Soloway P.C.
20090078560 - Devices, apparatus, methods and processes for generating hydrogen, oxygen and electricity from chemical compounds without producing undesirable by-products: Advantageously, virtually no undesirable by-products are produced, thus yielding environmentally friendly sources of fuels and energy. Through the cyclic use and re-use of acidic compounds, and especially sulfuric acid, water is processed to produce hydrogen, oxygen and electricity. One or more of the hydrogen, oxygen and electrical output of the... Agent: Gary L. Shaffer
20090078561 - Apparatus and methods for growing nanofibres and nanotips: This invention relates to heating apparatus and methods with particular applications for growing a nanofibre, and to nanotips fabricated by such methods and apparatus. Embodiments of the invention can be implemented to provide nanotips for electron gun sources and scanning probe microscopy. A nanotip fabrication apparatus includes a heater for... Agent: Tarolli, Sundheim, Covell & Tummino L.L.P.
20090078562 - Method of system maintenance planning based on continual robot parameter monitoring: At least one substrate location sensor is provided on a piece of equipment containing two adjoined chambers between which substrates may be transferred one at a time. Deviation of substrate position from a predetermined optimal position is measured as a substrate is transferred between the two adjoined chambers. Measured data... Agent: Scully, Scott, Murphy & Presser, P.C.
20090078563 - Plasma processing apparatus and method capable of adjusting temperature within sample table: A plasma processing method includes mounting a workpiece to be processed on an upper surface of a sample table disposed at a lower portion of an interior of a processing chamber disposed within a vacuum vessel and processing the workpiece by use of plasma formed within the processing chamber while... Agent: Antonelli, Terry, Stout & Kraus, LLP
20090078564 - Target structure and target holding apparatus: A target structure is provided which enables sputtering of gallium or gallium-containing material in a molten state to be achieved even when the film deposition rate is increased by increasing the input electric power. A sputtering apparatus including such a target structure is also provided. The target structure includes: a... Agent: Fitzpatrick Cella Harper & Scinto
20090078565 - Method and apparatus for depositing a coating onto a substrate: The present invention relates to a method for depositing a coating onto a substrate. The method comprises depositing by arc evaporation; depositing by dual magnetron sputtering; said depositing being performed in sequence or simultaneously.... Agent: Drinker Biddle & Reath (dc)
20090078566 - Deposited film forming method, deposited film forming device, deposited film, and photosensitive member provided with the deposited film: The present invention relates to a method of forming a deposited film including a first step for setting a deposited film forming target (10) into a reaction chamber (4), a second step for filling the reaction chamber (10) with a reaction gas and a third step for applying pulse DC... Agent: Hogan & Hartson L.L.P.
20090078567 - Method of connecting electrodes and hydrogen generating apparatus using the same: A method of connecting electrodes in a hydrogen generating apparatus and a hydrogen generating apparatus using this method are disclosed. The method of connecting the electrodes of a hydrogen generating apparatus may include: depositing a first terminal layer onto one side of a first electrode, which is configured to generate... Agent: Staas & Halsey LLP
20090078568 - On-demand hydrogen gas generation device having gas management system: The present disclosure generally relates to an on-demand hydrogen gas generation device, suitable for use in a fuel cell, which utilizes water electrolysis, and more particularly galvanic cell corrosion, and/or a chemical hydride reaction, to produce hydrogen gas. The present disclosure additionally relates to such a device that comprises a... Agent: Christopher M. Goff (27860) Armstrong Teasdale LLP
20090078569 - Inductively coupled plasma processing apparatus: An inductively coupled plasma processing apparatus according to the present invention prevents debris formed through a sputter etching operation from forming a film on an inner face of a side wall part 14 of a dielectric wall container 11 and a high-frequency power from being hindered to be supplied. All... Agent: Fitzpatrick Cella Harper & Scinto
20090078570 - Target/backing plate constructions, and methods of forming target/backing plate constructions: Target/backing plate constructions and methods of forming target/backing plate constructions are disclosed herein. The targets and backing plates can be bonded to one another through an appropriate interlayer. The targets can comprise one or more of titanium, tantalum, titanium zirconium, hafnium, niobium, vanadium, tungsten, copper or a combination thereof. The... Agent: Honeywell International Inc.
20090078571 - Magnet assembly capable of generating magnetic field having direction that is uniform and can be changed and sputtering apparatus using the same: The magnet assembly includes one rotatable dipole magnet subassembly, which is formed from a permanent magnet and a magnetically permeable convex end portion coupled to each of both ends of the permanent magnet, and at least two magnetically permeable flux guide subassemblies, which are configured so as to be magnetically... Agent: Fitzpatrick Cella Harper & Scinto
20090078572 - Magnetron end-block with shielded target mounting assembly: A magnetron arrangement includes an end block, which has a target fastening device for rotatable coupling of a tubular target, a holding device for a magnet system arranged in the interior of the tubular target and a shield, which covers the end of a tubular target mounted in the target... Agent: Heslin Rothenberg Farley & Mesiti PC
20090078573 - Solid-electrolyte gas sensor element, including a pump cell and a reference gas channel: A sensor element for determining gas components in measuring gas mixtures, particularly gas components in exhaust gases of combustion devices, having a measuring chamber that is in gas-conducting connection with the measuring gas mixture, and having a solid electrolyte which connects a pump electrode, situated in the measuring chamber, and... Agent: Kenyon & Kenyon LLP
20090078574 - Charge tags and the separation of nucleic acid molecules: The present invention relates to novel phosphoramidites, including positive and neutrally charged compounds. The present invention also provides charge tags for attachment to materials including solid supports and nucleic acids, wherein the charge tags increase or decrease the net charge of the material. The present invention further provides methods for... Agent: Casimir Jones, S.c.03/19/2009 > patent applications in patent subcategories.
20090071815 - Method and apparatus for selectively severing and analyzing non-covalent and other bonds of biological macromolecules: A biological sample solution is ionized by electrospray and the sample solution is irradiated with an infrared laser beam to dissociate biological macromolecules into the constituents thereof. As a result, only non-covalent bonds of the biological macromolecules can be selectively severed and analyzed.... Agent: Dickstein Shapiro LLP
20090071816 - Radio frequency plasma-water dissociator: A radio frequency plasma-water dissociator incorporates a plasma boiler, a RF Conduit, a dummy load, and a magnetron. The plasma boiler is in communication with the RF Conduit. The RF Conduit is in communication with the dummy load. And the dummy load is in communication with the magnetron. The magnetron... Agent: Law Offices Of Andrew Schroeder
20090071817 - Selective resonance of chemical structures: Chemical compositions may be selectively or preferentially excited by the application of scores comprising a series of energy inputs.... Agent: Searete LLC Clarence T. Tegreene
20090071818 - Film deposition apparatus and method of film deposition: An ion beam sputtering film deposition apparatus is provided which can form a high-quality thin film that is dense, smooth and faultless. The film deposition apparatus has ion beam irradiating unit, a target 105 containing a film forming substance to be sputtered, and holding unit 112 to hold a substrate... Agent: Fitzpatrick Cella Harper & Scinto
20090071819 - Electrolyzer cell stack system: Some embodiments of the present invention provide a balance-of-plant system and apparatus suited for regulating the operation of an electrolyzer cell stack. Specifically, in some embodiments, a balance-of-plant system and apparatus is operable to regulate the respective pressures of at least two reaction products relative to one another. Various examples... Agent: Bereskin And Parr
20090071820 - Ion exchange membrane electrolytic cell: [Means for Solving] A cushion material 10 is accommodated between a cathode gas chamber back plate 9 and a gas diffusion electrode 7 of an ion exchange membrane electrolytic cell 1 such that a repulsive force of the cushion material at the bottom part of the cathode gas chamber is... Agent: Ostrolenk Faber Gerb & Soffen
20090071822 - Alloy and sputtering target material for soft-magnetic film layer in perpendicular magnetic recording medium, and method for producing the same: There are provided a sputtering target material for a soft-magnetic film layer with a high saturation magnetic flux density and high amorphous properties and a method for producing the sputtering target material. The target material is made of an alloy comprising one or more of Zr, Hf, Nb, Ta and... Agent: The Webb Law Firm, P.C.
20090071821 - Sb-te alloy powder for sintering, sintered compact sputtering target obtained by sintering said powder, and manufacturing method of sb-te alloy powder for sintering: Provided is Sb—Te alloy powder for sintering in which the maximum grain size of the powder obtained by subjecting gas atomized powder of an Sb—Te alloy to mechanical pulverization is 90μm or less, and a sintered compact sputtering target obtained by sintering this powder. Further provided is a manufacturing method... Agent: Howson And Howson
20090071823 - Disposable enzymatic sensor for liquid samples: The present invention relates to a disposable electrochemical sensor which can measure redox species in a liquid sample... Agent: Unilever Patent Group
20090071824 - Integrated sensing array for producing a biofingerprint of an analyte: An integrated array of electronic sensing elements outputs a bio-fingerprint of an analyte. System is preferably constructed of as a series of three layers but need not be so arranged. An upper layer defines a fluid volume or analyte chamber; a middle layer contains the sensing elements; and a third... Agent: Diederiks & Whitelaw, PLC
20090071825 - Gas sensor designed to ensure stability of waterproofing of air flow path: A gas sensor equipped with an elastic member which is disposed hermetically in an open end of an air cover joined to a housing. The elastic member has a vertical hole, an air flow path, and lead-retaining holes through which leads pass to establish electric connections between a sensing device... Agent: Nixon & Vanderhye, PC
20090071826 - Anion concentration measuring device and anion concentration measuring element: The present invention aims to simplify the structure and a fabrication method of an ion-selective electrode in an ion concentration measuring device that measures an anion, particularly a chloride ion, in a biological component. To this end, in a potential difference measuring unit, a quaternary ammonium salt derivative serving as... Agent: Stanley P. Fisher Reed Smith LLP
20090071827 - Method and apparatus to reduce false positive and false negative identifications of compounds: A method, computer program medium, and system for analyzing a protein sample that obtains a mass spectrum of the derived peptides, and determines from the mass spectrum a first set of peptide identifications for the peptides. In the method, computer program medium, and system, incorrect identifications can be filtered from... Agent: Oblon, Spivak, Mcclelland Maier & Neustadt, P.C.
20090071828 - Devices exhibiting differential resistance to flow and methods of their use: The invention features microfluidic devices that contain structures that impart differential resistance to a fluid flow. The structures are disposed adjacent to intersections of channels. Devices of the invention provide differential resistance, e.g., under electric-field-driven flow and pressure-driven flow.... Agent: Clark & Elbing LLP
20090071829 - radio frequency identifiers for use in biological science: Provided herein are biological research methods, kits, and products that utilize radio frequency identifier technology.... Agent: Invitrogen Corporation C/o Intellevate
20090071830 - Systems and methods for isolating nucleic acids: A system for collecting target nucleic acids from a sample can include at least one sample chamber configured to receive a sample containing target nucleic acids and other material, at least one collection chamber removably mountable relative to the at least one sample chamber and configured to collect target nucleic... Agent: Mila Kasan, Patent Dept. Applied Biosystems
20090071831 - Methods and systems for producing arrays of particles: The invention provides apparatus and methods for arraying particles on a surface using dielectrophoresis.... Agent: Edwards Angell Palmer & Dodge LLP
20090071833 - Method and device for manipulating liquids in microfluidic systems: The present invention relates to microfluidic systems having components with specially designed and fabricated areas of enhanced and/or reduced capillarity (flow guides). The methods and devices of the present invention permit the bubble-less dispensing and mixing of small volumes of different liquids for subsequent incubation and/or detection of products of... Agent: Peter G. Carroll Medlen & Carroll, LLP
20090071832 - Microfluidic device with vertical injection aperture: A microfluidic device with a vertical injection aperture is provided. The microfluidic device comprises a separation channel, an injection aperture disposed adjacent to and in fluid communication with the separation channel. The microfluidic device further comprises a semi-permeable filter disposed adjacent to the injection aperture, wherein the filter is configured... Agent: General Electric Company Global Research
20090071834 - Methods and devices for concentration and fractionation of analytes for chemical analysis including matrix-assisted laser desorption/ionization (maldi) mass spectrometry (ms): A device is described for pre-concentration and purification of analytes from biological samples (such as human serum, plasma, homogenized solid tissue, etc.) to be analyzed by Matrix-Assisted Laser Desorption Ionization Mass Spectrometry (MALDI MS) and methods of use thereof are provided.... Agent: Mcdonnell Boehnen Hulbert & Berghoff LLP03/12/2009 > patent applications in patent subcategories.
20090065348 - Method of arc ion plating and target for use therein: It is an object of the present invention to provide an arc ion plating method and a target used therein, capable of obtaining a uniform film thickness distribution substantially throughout the overall length of a work and also capable of improving the yield of the target material and reducing the... Agent: Oblon, Spivak, Mcclelland Maier & Neustadt, P.C.
20090065350 - Filtered cathodic arc deposition with ion-species-selective bias: A dual-cathode arc plasma source is combined with a computer-controlled bias amplifier to synchronize substrate bias with the pulsed production of plasma. Accordingly, bias can be applied in a material-selective way. The principle has been applied to the synthesis metal-doped diamond-like carbon films, where the bias was applied and adjusted... Agent: Fliesler Meyer LLP
20090065349 - Plasma vapor deposition: A plasma vapor deposition system is described for forming a feature on a semiconductor wafer. The plasma vapor deposition comprises a primary target electrode and a plurality of secondary target electrodes. The deposition is performed by sputtering atoms off the primary and secondary target electrodes.... Agent: Slater & Matsil LLP
20090065351 - Method and apparatus for deposition: A deposition system supplies a continuous flow of process gases and sequentially selects among the flowing process gases for delivery to a reaction chamber. In the reaction chamber the delivered process gas acts as an ionizing species and thereby effects the deposition of a target substance upon a substrate. Gases... Agent: James Wiegand
20090065352 - Electrolyzing device: An electrolyzing device includes a first main electrode 3, a second main electrode 4, an auxiliary electrode 5, and control means C for controlling current supply to the electrodes, the control means C includes an electrolyzing mode in which treated water is electrochemically treated by using the first main electrode... Agent: Mcdermott Will & Emery LLP
20090065353 - Ionic foot bath array with ionic circulation: An ionic foot bath array for generating an ionic foot bath includes an upper rod support structure, at least one electrically non-conductive support structure leg depending downwards from the upper rod support structure and a plurality of generally cylindrical electrically conductive ionic rods each having the same diameter, the ionic... Agent: Adam H. Jacobs Law Offices Of Adam H. Jacobs
20090065354 - Sputtering targets comprising a novel manufacturing design, methods of production and uses thereof: A sputtering target is described herein, which includes: a) a surface material, and b) a core material coupled to the surface material, wherein at least one of the surface material or the core material has less than 100 ppm defect volume. Methods for producing sputtering targets are described that include:... Agent: Buchalter Nemer
20090065355 - Biosensor capable of simultaneous detection of substrate binding and reaction product: An object of the present invention is to provide a biosensor that can detect binding of a compound with a functional protein and then assay a reaction product derived from the activity of the functional protein again. The present invention provides a biosensor for detecting a test molecule specifically binding... Agent: Sughrue Mion, PLLC
20090065356 - Biosensor: In a biosensor for measuring glucose in a liquid sample, an additive agent which is one of an organic acid or organic acid salt having at least one carboxyl group in a molecule, an organic acid or organic acid salt having at least one amino group or carbonyl group in... Agent: Wenderoth, Lind & Ponack L.L.P.
20090065357 - Assay cartridges and methods of using the same: Assay modules, preferably assay cartridges, are described as are reader apparatuses which may be used to control aspects of module operation. The modules preferably comprise a detection chamber with integrated electrodes that may be used for carrying out electrode induced luminescence measurements. Methods are described for immobilizing assay reagents in... Agent: Scully Scott Murphy & Presser, PC
20090065358 - Oxygen sensor, and internal combustion engine and transport apparatus provided with the oxygen sensor: An oxygen sensor which is highly waterproof in a high-temperature environment and yet allows for downsizing includes a sensor element having a detection section arranged to detect oxygen, a housing, the sensor element being inserted at one end thereof in such a manner that the detection section is exposed, a... Agent: Yamaha Hatsudoki Kabushiki Kaisha C/o Keating & Bennett, LLP
20090065359 - Discrete contact mr bio-sensor with magnetic label field alignment: The invention describes a family of sensors for assaying macro-molecules and/or biological cells in solution. Each sensor has the form of a well (a hollow cylinder having a floor but no lid) or a trench whose walls comprise a plurality of GMR or TMR devices. Suitably shaped magnets located below... Agent: Saile Ackerman LLC
20090065360 - Multi-component, simultaneous, independent multi-gradient system for liquid chromatography: Systems and methods for separating charged molecules on the basis of their differential electrostatic binding to a charged stationary phase comprise controlling the creation of simultaneous independent or dependent pH and additive gradients.... Agent: Cooley Godward Kronish LLP Attn: Patent Group03/05/2009 > patent applications in patent subcategories.
20090057130 - Method of manufacturing particle wire: P
20090057131 - Direct injection of plasma activated species (pas) and radiation into liquid solutions assisted with by a gas buffered housing: A method of stimulating chemical reactions within a liquid uses a gas plasma ejected from a gas-buffered plasma injection device to create a plasma-liquid interface. The injection device has an electrically-conductive housing with an inlet, an outlet and an electrode embedded in the housing interior so as to create flow... Agent: Greenberg Traurig, LLP
20090057132 - Zinc oxide thin film, transparent conductive film and display device using the same: A zinc oxide thin film having desired crystallinity is fabricated. The present invention provides a zinc oxide thin film which laminated on a substrate, and which is a crystalline thin film of a wurtzite form. The c-axis of the crystalline thin film is oriented in a direction substantially perpendicular to... Agent: Antonelli, Terry, Stout & Kraus, LLP
20090057133 - Method and apparatus for reactive solid-gas plasma deposition: A device for magnetically enhanced sputtering and plasma deposition includes a plasma source unit and a work piece processing unit in which an anode space and a processing chamber are located in direct communication with each other. Sputtering and reactive gases are provided through an inlet of the processing chamber... Agent: Nixon & Vanderhye, PC
20090057134 - Thin film application device and method for coating small aperture vacuum vessels: A device and method for coating an inside surface of a vessel is provided. In one embodiment, a coating device comprises a power supply and a diode in electrical communication with the power supply, wherein electrodes comprising the diode reside completely within the vessel. The method comprises reversibly sealing electrodes... Agent: Cherskov & Flaynik The Civic Opera Building
20090057135 - Sputtering method and apparatus: The sputtering apparatus includes a vacuum vessel, a sputter electrode placed within the vacuum vessel to hold a target material to be sputtered, a radio frequency power source for applying radio frequency waves to the electrode, a substrate holder which is spaced from the electrode and on which a substrate... Agent: Birch Stewart Kolasch & Birch
20090057136 - Manufacturing method for thin film battery: A thin film battery manufacturing method is provided for deposition of lithium metal oxide films onto a battery substrate. The films are deposited in a sputtering chamber having a plurality of sputtering targets and magnetrons. The sputtering gas is energized by applying a voltage bias between a pair of the... Agent: Janah & Associates A Professional Corp
20090057137 - Synthesizing thin films of lithiated transition metal oxide for use in electrochemical and battery devices: A method (100) is provided for synthesizing a thin film electrode (350) such as an electrochromic (EC) electrode (426) or counter electrode (434) for an EC device (410), a lithiated film of transition metal oxide (616) for a battery device (600), or the like. The method (100) includes providing (140)... Agent: Paul J White, Patent Counsel National Renewable Energy Laboratory (nrel)
20090057138 - Surface treatment installation for metallic parts, particularly by electrolysis: Surface treatment installation (100) for metallic parts including an electrolytic cell (1) comprising a treatment liquid (20) in which the parts to be treated are immersed, characterised in that the parts to be treated are fixed on a pivoting drum (2) such that there is at least one rotation movement... Agent: Frommer Lawrence & Haug
20090057140 - Ag base alloy sputtering target and method for manufacturing the same: (2) the ratio of the total area of Cu particles having a circle equivalent diameter of from 10 μm or more to 50 μm or less, to the total area of all Cu particles, is 70% or more, and the average distance between the centers of gravity is from 60... Agent: Oblon, Spivak, Mcclelland Maier & Neustadt, P.C.
20090057141 - Ag-based alloy sputtering target: The invention relates to an Ag-based alloy sputtering target including at least one element selected from the group consisting of Ti, V, W, Nb, Zr, Ta, Cr, Mo, Mn, Fe, Co, Ni, Cu, Al, and Si in a total amount of 1 to 15% by weight, in which the Ag-based... Agent: Oblon, Spivak, Mcclelland Maier & Neustadt, P.C.
20090057143 - Film-depositing target and preparation of phase shift mask blank: A film-depositing target for use in the manufacture of a halftone phase shift mask blank includes a transparent substrate and a translucent film of one or more layers having a controlled phase and transmittance, at least one layer of the translucent film including silicon, molybdenum and zirconium at the same... Agent: Birch Stewart Kolasch & Birch
20090057142 - Hafnium alloy target and process for producing the same: A hafnium alloy target containing either or both of Zr and Ti in a gross amount of 100 wtppm-10 wt % in Hf; wherein the average crystal grain size is 1-100 μm, the impurities of Fe, Cr and Ni are respectively 1 wtppm or less, and the habit plane ratio... Agent: Howson And Howson
20090057139 - Pot-shaped copper sputtering target and manufacturing method thereof: Provided is a pot-shaped copper sputtering target manufactured with die forging, wherein the Vickers hardness Hv at all locations of the inner surface of the pot-shaped target is 70 or greater. With this pot-shaped copper sputtering target, the average crystal grain size in the target structure is 65 μm or... Agent: Howson And Howson
20090057144 - Arc evaporation source and vacuum deposition system: An arc evaporation source and a vacuum deposition system capable of properly collecting an evaporated material emitted from a cathode in vacuum arc discharge are provided. An arc evaporation source (100) includes a first electrode and a second electrode (14A, 14B) disposed so as to face each other with a... Agent: Marshall, Gerstein & Borun LLP
20090057145 - Apparatus for monitoring chlorine concentration in water: Apparatus (2) for monitoring chlorine in water (4), which apparatus (2) comprises a flow cell (6), the flow cell (6) containing a chlorine sensor (62) and an automatic calibration system, and the automatic calibration system being such that it comprises a small pair of in-line electrodes (50) for generating low... Agent: Iandiorio Teska & Coleman
20090057146 - Analyte test strip with improved reagent deposition: An analyte, system, strip and method are described. In one example, an analyte test strip is provided that includes a substrate, electrically conductive material and an isolated portion of the electrically conductive material. The substrate has a generally planar surface that extends from a first end to a second end.... Agent: Philip S. Johnson Johnson & Johnson
20090057147 - Devices and methods for biochip multiplexing: The invention is directed to devices that allow for simultaneous multiple biochip analysis. In particular, the devices are configured to hold multiple cartridges comprising biochips comprising arrays such as nucleic acid arrays, and allow for high throughput analysis of samples.... Agent: Morgan, Lewis & Bockius, LLP
20090057148 - In vivo analyte monitor with malfunction detection: The measuring system for in vivo monitoring of an analyte concentration with malfunction detection, comprises an electrode system, a potentiostat and an evaluation unit. The electrode system has a working electrode, a reference electrode, and a counter electrode. The potentiostat is for adjusting a difference of potential between the electric... Agent: Roche Diagnostics Operations Inc.
20090057149 - Method of manufacturing a diagnostic test strip: A method for manufacturing a biosensor is provided. The method may include positioning a shadow mask containing a pattern of a plurality of feature sets over a substantially planar base layer containing a plurality of registration points. The method may also include forming at least one of the plurality of... Agent: Finnegan, Henderson, Farabow, Garrett & Dunner LLP
20090057150 - Electrochemical gas sensor: An electrochemical gas sensor is disclosed which comprises a gas sensing electrode and a counter electrode disposed within a housing, the housing having an aperture for gas ingress, the gas sensing electrode and counter electrode being separated by a region containing electrolyte, and means for connecting the gas sensing electrode... Agent: Honeywell International Inc.Previous industry: Distillation: processes, separatory
Next industry: Electrolysis: processes, compositions used therein, and methods of preparing the compositions
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